4-氨基-3-戊烯-2-酮合成路线 (共 77 条)
反应条件
in water addn. of 4-amino-3-penten-2-one to aq. soln. of nickel compd.; isolation of ppt., recrystn. (CHCl3), elem. anal.;
参考文献
Jamialahmadi; Tayyari; Habibi; Yazdanbakhsh; Sammelson
Journal of Molecular Structure, 2011 , vol. 997, # 1-3 p. 117 - 125
参考文献
Combes,A.; Combes,C.
Bulletin de la Societe Chimique de France, 1892 , vol. <3> 7, p. 791
反应条件
copper acetylacetonate in dichloromethane T=55 - 60°C; 72 h;
参考文献
Augusti, Rodinei; Eberlin, Marcos N.; Kascheres, Concetta
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1355 - 1358
反应条件
acetic acid in ethanol T=20°C; 24 h;
参考文献
Heterocycles, , vol. 55, # 2 p. 331 - 352
反应条件
ammonium acetate; acetic acid
参考文献
Franke; Kraft
Angewandte Chemie, 1955 , vol. 67, p. 395,398
参考文献
Dornow
Chemische Berichte, 1939 , vol. 72, p. 1548
反应条件
1: ethanol 2: 120 °C View Scheme
参考文献
Bohlmann; Rahtz
Chemische Berichte, 1957 , vol. 90, p. 2265,2270
参考文献
Baumgarten; Dornow
Chemische Berichte, 1939 , vol. 72, p. 563,566
Full Text Show Details
Dornow; Schacht
Chemische Berichte, 1949 , vol. 82, p. 117,119
Full Text Show Details
Dornow
Chemische Berichte, vol. 72, p. 1550
反应条件
1: 160 - 165 °C 2: concentrated alkali View Scheme
参考文献
Knoevenagel; Cremer
Chemische Berichte, 1902 , vol. 35, p. 2394
反应条件
1: 100 - 110 °C / reagiert analog mit 3-Aethoxy-crotonaldehyd-diaethylacetal
2: sulfur; dioxane; aqueous <NH4>2S / 175 - 180 °C
3: P2O5
4: platinum; H2O / Hydrogenation
5: aqueous sulfuric acid; aqueous sodium nitrite
View Scheme
参考文献
Dornow; Schacht
Chemische Berichte, 1949 , vol. 82, p. 117,119