sodium hydride in N,N-dimethyl-formamide T=80 - 90°C; 12 h;
参考文献
Salunkhe, A. M.; Phadke, A. S.; Kulkarni, Sheshgiri N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1172 - 1173
Salunkhe, A. M.; Phadke, A. S.; Kulkarni, Sheshgiri N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1172 - 1173
1: 20 percent / NaH / dimethylformamide / 24 h / 80 - 90 °C
2: 91 percent / NaCl, H2O / dimethylsulfoxide / 5 h / 150 - 160 °C
3: 70 percent / Na, EtOH / tetrahydrofuran / 0-5 deg C, 2 h, then RT, 3 h
View Scheme
参考文献
Salunkhe, A. M.; Phadke, A. S.; Kulkarni, Sheshgiri N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1172 - 1173
