反应条件
With Na{HB(OMe)3} in tetrahydrofuran addn of Na{HB(OMe)3} to cis-chloro(methyl){bis(dicyclohexylphosphino)ethane}platinum(II) in THF with immediate cloudiness, after 3 h quenched by aq.NH4Cl; layers sepd., aq. layer extrd. with ether, solvent removal by evapn., resulting oil dissolved in min. of THF, 4 parts methanol added, crystn. at -10°C, suction filtrn.;
参考文献
Hackett, Marifaith; Whitesides, George M. Journal of the American Chemical Society, 1988 , vol. 110, # 5 p. 1449 - 1462