1.1: morpholine / n-heptane; water / 1 h / 0 - 20 °C 1.2: 20 h / 45 °C 1.3: 2 h / 20 °C 2.1: isopropyl alcohol / 1 h / 20 °C 3.1: hydrogen / methanol / 29422.9 Torr / autoclave View Scheme
1.1: morpholine / n-heptane; water / 1 h / 0 - 20 °C 1.2: 20 h / 45 °C 1.3: 2 h / 20 °C 2.1: isopropyl alcohol / 1 h / 20 °C 3.1: hydrogen / methanol / 29422.9 Torr / autoclave View Scheme
Gitterman, Amy; Parry, Ronald J.; Dufresne, Richard F.; Sternbach, Daniel D.; Cabelli, Michael D.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2074 - 2081
1.1: morpholine / n-heptane; water / 1 h / 0 - 20 °C
1.2: 20 h / 45 °C
1.3: 2 h / 20 °C
2.1: isopropyl alcohol / 1 h / 20 °C
3.1: hydrogen / methanol / 29422.9 Torr / autoclave
View Scheme