1.1: NaH / dimethylformamide / 1 h / 20 °C 1.2: 83 percent / dimethylformamide / 3 h / 20 °C 2.1: 64 percent / NaBH4; HCl / 2 h / -10 °C View Scheme
参考文献
Tarling, Chris A.; Holmes, Andrew B.; Markwell, Roger E.; Pearson, Neil D.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1695 - 1701
1: sodium sulphite / H2O / Heating 2: phosphorus trichloride oxide / 120 - 140 °C 3: 17 percent / 2,2'-azoisobutyronitrile / CuCl2 / 0.5 h / 170 °C 4: 1,8-diazabicyclo<5.4.0>undec-7-ene / benzene / 1.5 h / Heating View Scheme
参考文献
Culshaw, Peter N.; Walton, John C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 8 p. 1201 - 1208