1,4-二氰基-2-丁烯合成路线 (共 11 条)
反应条件
tetramethyl-1,1,3,3 disila-1,3 cyclobutane; tungsten hexachloride in benzene T=60°C; 10 h;
参考文献
Bespalova, N. B.; Bovina, M. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.2 p. 156 - 159
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 172 - 176
反应条件
ruthenium in dichloromethane 2 h; Heating; Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 7, # 11 p. 2113 - 2116
反应条件
tetramethyl-1,1,3,3 disila-1,3 cyclobutane; tungsten tetrachloride in benzene T=60°C; P=0.001 Torr; 10 h; other temperature; metathesis of allyl cyanide;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 799 - 800
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 920 - 921
反应条件
hydrogenchloride; copper; copper(l) chloride; sodium chloride
参考文献
Justus Liebigs Annalen der Chemie, , vol. 631, p. 21 - 56
反应条件
Ph2POiPr; isopropyl alcohol in toluene T=60°C; other phosphinite catalysts; activation parameters (EA, ΔS(act., 298 K); kinetics and mechanism of the phosphinite-catalyzed dimerization of acrylonitrile; Rate constantEquilibrium constantThermodynamic data;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 109, # 1-4 p. 521 - 524
反应条件
aluminum oxide; rhenium(VII) oxide on aluminum oxide; tetraethyl tin; tetramethylstannane 24 h; Ambient temperatureheterogeneous self-metathesis, co-metathesis; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 262 - 263
反应条件
1: potassium cyanide; pyridine / 80 °C 2: aqueous hydrochloric acid / 140 °C View Scheme
参考文献
Piepenbrink
Justus Liebigs Annalen der Chemie, 1951 , vol. 572, p. 83,91
反应条件
hydrogen; (o-OC6H4CH3)3PRuCl(PPh3)2 T=130°C; P=3620.04 Torr; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 743
反应条件
ammonia; water; hydrogen; cobalt
参考文献
Du Pont de Nemours and Co.
Patent: US2532277 , 1948 ;