1: 97 percent / Cs2CO3, KI / acetone / 18 h / Heating 2: 80 percent / H2 / PtO2 / ethanol / 0.5 h / 1810.02 Torr 3: 33 percent / Et3N / CH2Cl2 / 2 h / -70 deg C to 10 deg C View Scheme
参考文献
Musser, John H.; Kreft, Anthony F.; Bender, Reinhold H. W.; Kubrak, Dennis M.; Carlson, Richard P.; et al.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1176 - 1183
1: 97 percent / Cs2CO3, KI / acetone / 18 h / Heating 2: 80 percent / H2 / PtO2 / ethanol / 0.5 h / 1810.02 Torr 3: 33 percent / Et3N / CH2Cl2 / 2 h / -70 deg C to 10 deg C View Scheme
参考文献
Musser, John H.; Kreft, Anthony F.; Bender, Reinhold H. W.; Kubrak, Dennis M.; Carlson, Richard P.; et al.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1176 - 1183
triethylamine in dichloromethane 2 h; -70 deg C to 10 deg C;
参考文献
Musser, John H.; Kreft, Anthony F.; Bender, Reinhold H. W.; Kubrak, Dennis M.; Carlson, Richard P.; et al.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1176 - 1183
