反应条件
1: Wang resin-bound Fmoc-L-glutamic acid With piperidine in N,N-dimethyl-formamide T=20°C; 2: dodecanoyl chloride With N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 1 h; 3: With trifluoroacetic acid in dichloromethane T=20°C; 18 h;
参考文献
Phoon, Chee Wee; Somanadhan, Brinda; Heng, Sabrina Cher Hui; Ngo, Anna; Ng, Siew Bee; Butler, Mark S.; Buss, Antony D.; Sim, Mui Mui
Tetrahedron, 2004 , vol. 60, # 50 p. 11619 - 11628