反应条件
1: 1.) Et3N, glacial acetic acid, NaI, 2.) KI / 1.) dichloromethane, 0 deg C, 30 min; 2.) reflux, 1 h
2: 1.) NaBH4, glacial acetic acid, 2.) HCl, HCHO / 1.) ethanol, water, 0 deg C, 2 h; 2.) 80 deg C, 10 min
View Scheme
参考文献
Doleschall, Gabor; Seres, Peter
Acta Chimica Hungarica, 1987 , vol. 124, # 2 p. 209 - 216
