1,2-二(2-氯乙氧基)乙烷合成路线 （共 69 条）
反应条件
lithium hydroxide in water; butan-1-ol modified Pedersen procedure; 28 h; Heating;
参考文献
Dalton Transactions, , # 27 p. 2915 - 2924
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
反应条件
lithium hydroxide in water; butan-1-ol modified Pedersen procedure; 28 h; Heating;
参考文献
Dalton Transactions, , # 27 p. 2915 - 2924
反应条件
sodium hydroxide; lithium perchlorate 1.) DMSO, 60 deg C, 15 min, 2.) 110 deg C, 22 h; Yield given. Multistep reaction;
参考文献
Pacey, G. E.; Wu, Y. P.; Bubnis, B. P.
Synthetic Communications, 1981 , vol. 11, # 4 p. 323 - 328
反应条件
potassium hydroxide T=140°C; 120 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fenton, David E.; Parkin, Donald; Newton, Roger F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 449 - 454
反应条件
tri-n-butylhexadecylphosphonium bromide in toluene T=100°C; 10 h;
参考文献
Ciuffarin, Ennio; Isola, Mauro; Leoni, Piero
Journal of Organic Chemistry, 1981 , vol. 46, # 15 p. 3064 - 3070
反应条件
potassium hydroxide 0.166667 h; microwave irradiation;
参考文献
Ziafati, Ahmad; Sabzevari, Omolbanin; Heravi, Majid M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 4 p. 803 - 807
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
反应条件
1: 99 percent / NaN3 / NaI / acetonitrile / 48 h / Heating 2: 77 percent / PPh3; aq. HCl / diethyl ether; tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Feau, Clementine; Klein, Emmanuel; Kerth, Paul; Lebeau, Luc
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 6 p. 1499 - 1503
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
