1,2-二(2-氯乙氧基)乙烷合成路线 （共 69 条）
反应条件
sodium carbonate in xylene
48 h; Heating;
参考文献
Bradshaw, Jerald S.; An, Haoyun; Krakowiak, Krzysztof E.; Wang, Tingmin; Zhu, Chengyue; Izatt, Reed M.
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6112 - 6118
反应条件
lithium bromide; lithium tert-butylate
1.) tert-Butanol, reflux, 2.) reflux, ca. 12 d; Yield given. Multistep reaction;
参考文献
Gloe, K.; Muehl, P.; Beger, J.; Poeschmann, C.; Petrich, M.; Beyer, L.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 413 - 421
反应条件
sodium azide; sodium iodide in acetonitrile
48 h; Heating;
参考文献
Klein, Emmanuel; DeBonis, Salvatore; Thiede, Bernd; Skoufias, Dimitrios A.; Kozielski, Frank; Lebeau, Luc
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 19 p. 6474 - 6488
反应条件
sodium ditelluride in tetrahydrofuran
T=-78 - 20°C;
参考文献
Hesford, Matthew J.; Levason, William; Matthews, Melissa L.; Reid, Gillian
Dalton Transactions, 2003 , # 14 p. 2852 - 2858
反应条件
1: 45 percent / potassium hydroxide / 24 h / 100 °C
2: 42 percent / sodium hydroxide / tetrahydrofuran / 24 h / 66 °C
View Scheme
参考文献
Ouchi, Mikio; Inoue, Yoshihisa; Kanzaki, Takashi; Hakushi, Tadao
Journal of Organic Chemistry, 1984 , vol. 49, p. 1408 - 1412
参考文献
King,A.P.; Krespan,C.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 1315 - 1316
参考文献
King,A.P.; Krespan,C.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 1315 - 1316
反应条件
1: NaH
2: SOCl2, Py / benzene / Heating
View Scheme
参考文献
Prelog,V.; Bedekovic,D.
Helvetica Chimica Acta, 1979 , vol. 62, p. 2285 - 2303
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in toluene
Heating;
参考文献
Lukyanenko, Nikolai G.; Basok, Stepan S.; Filonova, Lyubov K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3141 - 3148
