反应条件
1: 26 percent / NaH / tetrahydrofuran / 48 h / Heating
2: 1.) BH3*(CH3)2S, 2.) aq. NaOH, 30percent H2O2 / 1a.) THF, 0 deg C, 2 h, 1b.) room temperature, 2 h, 2.) water, 50 deg C, 1 h
3: 1.) NaH / 1.) THF, room temperature, 1 h, 2.) room temperature
View Scheme
参考文献
Czech, Bronislaw P.; Babb, David A.; Son, Byungki; Bartsch, Richard A.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 4805 - 4810
