1: 50 percent / triethylamine / acetonitrile / 12 h / 20 °C
2: 100 percent / NaI / acetone / 5 h / Heating
View Scheme
参考文献
Markovskii, L. N.; Rudkevich, D. M.; Kal'chenko, V. I.; Tsymbal, I. F.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 11 p. 2094 - 2100
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 11 p. 2425 - 2433
1: 3 h / 760 Torr / slowly up to 180 deg C
2: 1) (NH4)2CO3, 2) N2O3 / 1) H2O, 16 h, 2) CH2Cl2
View Scheme
参考文献
Kellogg, Richard M.; Bergen, T. J. van; Doren, Henk van; Hedstrand, David; Kooi, J.; et al.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2854 - 2862
Bethell, Donald; Galsworthy, Peter J.; Jones, Keith
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 2035 - 2044