1-methyl-pyrrolidin-2-one; tetrabutylammomium bromide; nickel dichloride; buta-1,3-diene in tetrahydrofuran; hexane T=25°C; 48 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 45 p. 6180 - 6182
1: 1-bromo-butane With iodine; magnesium in diethyl ether T=60°C; 1 h; 2: 1-bromo-decane With 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; ferrous acetate in diethyl ether T=20°C; Kumada coupling reaction; 0.25 h; Further stages. Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1015 - 1018
