potassium carbonate in N,N-dimethyl-formamide T=60°C; 16 h; Inert atmosphere;
参考文献
Mysliwiec, Damian; Donnio, Bertrand; Chmielewski, Piotr J.; Heinrich, Benoit; Stepien, Marcin
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4822 - 4833
1: 1-bromo-butane With iodine; magnesium in diethyl ether T=60°C; 1 h; 2: 1-bromo-decane With 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; ferrous acetate in diethyl ether T=20°C; Kumada coupling reaction; 0.25 h; Further stages. Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1015 - 1018
