The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britian and Northern Ireland of Defence Evaluation and Research Agency
Patent: US6242636 B1, 2001 ;
1: hex-1-yne With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C;
2: 1-bromo-decane With tetra-(n-butyl)ammonium iodide in tetrahydrofuran
12 h; Heating;