1: With C2H6BrOS(1+) in dichloromethane
T=-78 - 0°C; 1 h; Inert atmosphereElectrochemical reaction;
2: With triethylamine in dichloromethane
T=0 - 25°C; 1 h; Inert atmosphereElectrochemical reaction;
参考文献
Ashikari, Yosuke; Shimizu, Akihiro; Nokami, Toshiki; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2013 , vol. 135, # 43 p. 16070 - 16073
N-bromosuccinmide; DME*5HF in dichloromethane
T=20°C; 3 h;
参考文献
Bucsi, Imre; Toeroek, Bela; Marco, Alfonso Iza; Rasul, Golam; Prakash, G. K. Surya; Olah, George A.
Journal of the American Chemical Society, 2002 , vol. 124, # 26 p. 7728 - 7736