1: 52 percent / potassium tert-butoxide / tetrahydrofuran / 13 h / Heating
2: 89 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
3: 81 percent / toluene / 12 h / Heating
4: 87 percent / H2, conc. HCl / 10percent Pd/C / ethanol / 12 h / 3102.9 Torr
5: 72 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
6: 90 percent / H2 / 10percent Pd/C / ethanol / 8 h / 2585.7 Torr
7: 48percent HBF4, NaNO2 / H2O / 0.17 h / 0 °C
8: NaOAc / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 24 h
View Scheme
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
1: 52 percent / potassium tert-butoxide / tetrahydrofuran / 13 h / Heating
2: 89 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
3: 81 percent / toluene / 12 h / Heating
View Scheme
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
1: 52 percent / potassium tert-butoxide / tetrahydrofuran / 13 h / Heating
2: 89 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
3: 81 percent / toluene / 12 h / Heating
4: 87 percent / H2, conc. HCl / 10percent Pd/C / ethanol / 12 h / 3102.9 Torr
5: 72 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
View Scheme
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
