反应条件
1: potassium hydroxide / dichloromethane / 5 h / 0 - 3 °C
2: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 80 °C
3: hydrogenchloride; triphenylphosphine / water; ethyl acetate / 12 h / 20 °C
4: N,N-dimethyl-formamide / 12 h / 20 °C
View Scheme
参考文献
Davila, Johanna; Chassepot, Armelle; Longo, Johan; Boulmedais, Fouzia; Reisch, Andreas; Frisch, Benoit; Meyer, Florent; Voegel, Jean-Claude; Mesini, Philippe J.; Senger, Bernard; Metz-Boutigue, Marie-Helene; Hemmerle, Joseph; Lavalle, Philippe; Schaaf, Pierre; Jierry, Loic
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 83 - 86