反应条件
1: 93 percent / Amberlyst H-15 / CH2Cl2 / 1 h / 0 °C 2: 91 percent / NaI / acetone 3: 1.) (i-C3H7)2NLi / 1.) THF, n-hexane, room temp., 3 h, 2.) 55 deg C, 12 h 4: 92 percent / Amberlyst H-15 / methanol / 1 h / 45 °C 5: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating 6: MnO2 / CH2Cl2 / 6 h / Ambient temperature 7: 1.) Mg/Hg / 1.) Et2O, 30 min, 2.) room temp., 1 h 8: 98 percent / pyridine / 1 h 9: 88 percent / N2H4*H2O, H2O2 / ethanol / 12 h / 50 - 60 °C View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 110, # 9/10 p. 523 - 526
