(Z)-十八碳-9-烯腈合成路线 （共 24 条）
反应条件
1: With diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; 3 h; Inert atmosphere;
2: With ammonia; iodine in tetrahydrofuran; hexane; dichloromethane; water
T=-78 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
1: With sodium diisobutyl-tert-butoxyaluminium hydride in tetrahydrofuran
T=0°C; 2 h; Inert atmosphere;
2: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; ammonia in tetrahydrofuran; water
T=0 - 20°C; 3 h;
参考文献
Suzuki, Yusuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 41 p. 7956 - 7962
反应条件
phosphorus pentoxide
T=150°C; 8 h;
参考文献
Barton; Jaszberenyi; Theodorakis
Tetrahedron, 1992 , vol. 48, # 13 p. 2613 - 2626
反应条件
in dichloromethane
T=0°C; Irradiation;
参考文献
Barton; Jaszberenyi; Theodorakis
Tetrahedron Letters, 1991 , vol. 32, # 28 p. 3321 - 3324
反应条件
in dichloromethane
T=0°C; Irradiation;
参考文献
Barton; Jaszberenyi; Theodorakis
Tetrahedron, 1992 , vol. 48, # 13 p. 2613 - 2626
反应条件
1: 95 percent / NH3(gas) / CH2Cl2 / 1 h / Ambient temperature
2: 95 percent / P2O5 / 8 h / 150 °C
View Scheme
参考文献
Barton; Jaszberenyi; Theodorakis
Tetrahedron, 1992 , vol. 48, # 13 p. 2613 - 2626
反应条件
1: (COCl)2, DMF / benzene / 3 h / Ambient temperature
2: 95 percent / NH3(gas) / CH2Cl2 / 1 h / Ambient temperature
3: 95 percent / NH3(gas) / CH2Cl2 / 1 h / Ambient temperature
4: 95 percent / P2O5 / 8 h / 150 °C
View Scheme
参考文献
Barton; Jaszberenyi; Theodorakis
Tetrahedron, 1992 , vol. 48, # 13 p. 2613 - 2626
反应条件
1: 95 percent / NH3(gas) / CH2Cl2 / 1 h / Ambient temperature
2: 95 percent / NH3(gas) / CH2Cl2 / 1 h / Ambient temperature
3: 95 percent / P2O5 / 8 h / 150 °C
View Scheme
参考文献
Barton; Jaszberenyi; Theodorakis
Tetrahedron, 1992 , vol. 48, # 13 p. 2613 - 2626
反应条件
ammonia; hydrogen; silica gel
T=370°C;
参考文献
I.G.Farbenind.
Patent: US2177619 , 1937 ;
参考文献
Sun Chem. Co.
Patent: US2444828 , 1946 ;
