反应条件
triethylamine in tetrahydrofuran
under Ar; soln. of iodoferrocene (0.5 mmol), PdCl2(PPh3)2 (0.025 or 0.05mmol), CuI (0.01 or 0.02 mmol) dissolved in THF, triethylamine (1 mmol) , and alkyne (0.5 or 1.25 mmol) added, atm. changed for CO, heated at 60°C for 12 h; solvent removed in vacuo, column chromy. (silica gel, toluene); elem. anal.;
参考文献
Feher, Csaba; Kuik, Arpad; Mark, Laszlo; Kollar, Laszlo; Skoda-Foeldes, Rita
Journal of Organometallic Chemistry, 2009 , vol. 694, # 25 p. 4036 - 4041
