反应条件
1: 77 percent / conc. hydrochloric acid / ethanol / 2.5 h / Heating
2: 1.) n-butyl-lithium / 1.) hexane, tetramethylethylenediamine, 25 deg C, 2 h, 2.) 0 deg C, 1 h
3: 89 percent / lithium aluminium hydride
4: 38 percent / phosphorus tribromide
5: 1.) n-butyl-lithium / 1.) hexane, hexamethylphosphoramide, THF, -78 deg C, 20 min, 2.) -78 deg C, 1 h
View Scheme
参考文献
Barker, Andrew J.; Pattenden, Gerald
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1901 - 1904
