lithium salt of proline; tetrabutylammomium bromide; potassium hydroxide; copper dichloride in water T=120°C; 0.666667 h; Microwave irradiationGreen chemistry;
1: thien-2-yl-lithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 3-iodo-pyridine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating; Further stages.;
参考文献
Font-Sanchis, Enrique; Cespedes-Guirao, F. Javier; Sastre-Santos, Angela; Fernandez-Lazaro, Fernando
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3589 - 3591
1: 3-iodo-pyridine With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 2 h; 2: With indium(III) chloride in tetrahydrofuran; pentane T=-78 - 20°C; 3: 2-Iodothiophene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; pentane Heating; Further stages.;
参考文献
Font-Sanchis, Enrique; Cespedes-Guirao, F. Javier; Sastre-Santos, Angela; Fernandez-Lazaro, Fernando
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3589 - 3591
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 7 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 11 p. 1159 - 1162
Khimiya Geterotsiklicheskikh Soedinenii, , # 11 p. 1467 - 1470
