您好,欢迎来到魔法化学网!
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-碘吡啶
合成路线
(共 228 条)
1120-90-7
3-碘吡啶
+
5188-07-8
甲硫醇钠
→
反应条件
18794-33-7
3-(甲基硫代)吡啶
反应条件
in 1-methyl-pyrrolidin-2-one T=100°C; 0.0416667 h; microwave irradiation;
参考文献
Cherng, Yie-Jia
Tetrahedron, 2002 , vol. 58, # 24 p. 4931 - 4935
1120-90-7
3-碘吡啶
+
536-74-3
苯乙炔
→
反应条件
13238-38-5
3-苯基乙炔吡啶
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine in water T=20°C; 30 h;
参考文献
Inoue, Naoki; Sugimoto, Osamu; Tanji, Ken-ichi
Heterocycles, 2007 , vol. 72, p. 665 - 671
1120-90-7
3-碘吡啶
+
2170-06-1
苯基乙炔基三甲基硅烷
→
反应条件
13238-38-5
3-苯基乙炔吡啶
反应条件
tetrabutyl-ammonium chloride; sodium acetate; tris-(o-tolyl)phosphine; palladium diacetate in N,N-dimethyl-formamide T=100°C; Sonogashira coupling; 0.25 h; microwave irradiation;
参考文献
Sorensen, Ulrik S.; Pombo-Villar, Esteban
Tetrahedron, 2005 , vol. 61, # 10 p. 2697 - 2703
1120-90-7
3-碘吡啶
+
591-50-4
碘苯
+
115-19-5
2-甲基-3-丁炔-2-醇
→
反应条件
13238-38-5
3-苯基乙炔吡啶
反应条件
1: iodobenzene; 2-methyl-but-3-yn-2-ol With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine T=50°C; 1 h; Inert atmosphere; 2: 3-iodo-pyridine With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium hydroxide T=110°C; 5 h; Inert atmosphere;
参考文献
Zhao, Yankai; Liu, Qiang; Li, Jing; Liu, Zhongquan; Zhou, Bo
Synlett, 2010 , # 12 p. 1870 - 1872
1120-90-7
3-碘吡啶
+
95-16-9
苯并噻唑
→
反应条件
2612-72-8
2-吡啶-3-基-1,3-苯并噻唑
反应条件
[2,2']bipyridinyl; [Ni(O2CCH3)2]*4H2O; Mg(O-t-Bu)2 in N,N-dimethyl-formamide T=100°C; 36 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
1120-90-7
3-碘吡啶
+
292638-84-7
→
反应条件
2633-06-9
3-苯乙烯基吡啶
反应条件
1: 3-iodo-pyridine With palladium diacetate; heptakis(6-deoxy-6-amino)β-CD in water; N,N-dimethyl-formamide 0.5 h; 2: styrene With potassium carbonate in water; N,N-dimethyl-formamide T=80°C; 5 h;
参考文献
Kanagaraj, Kuppusamy; Pitchumani, Kasi
Chemistry - A European Journal, 2013 , vol. 19, # 43 p. 14425 - 14431
1120-90-7
3-碘吡啶
+
72761-85-4
→
反应条件
2633-06-9
3-苯乙烯基吡啶
反应条件
potassium hydroxide; bis(dibenzylideneacetone)-palladium(0) in methanol T=70°C; 16 h; optical yield given as percent de;
参考文献
Sore, Hannah F.; Boehner, Christine M.; Laraia, Luca; Logoteta, Patrizia; Prestinari, Cora; Scott, Matthew; Williams, Katharine; Galloway, Warren R. J. D.; Spring, David R.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 504 - 515
1120-90-7
3-碘吡啶
→
反应条件
2633-06-9
3-苯乙烯基吡啶
反应条件
1: 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; potassium hydroxide; bis(dibenzylideneacetone)-palladium(0) / tert-butyl alcohol / 80 °C / Inert atmosphere 2: tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium(0) / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme
参考文献
Sore, Hannah F.; Boehner, Christine M.; Laraia, Luca; Logoteta, Patrizia; Prestinari, Cora; Scott, Matthew; Williams, Katharine; Galloway, Warren R. J. D.; Spring, David R.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 504 - 515
1120-90-7
3-碘吡啶
+
100-46-9
→
反应条件
2503-55-1
反应条件
tetraethylammonium chloride; molybdenum hexacarbonate in 1,4-dioxane T=130°C; 4 h; Microwave irradiation;
参考文献
Roberts, Bryan; Liptrot, David; Alcaraz, Lilian; Luker, Tim; Stocks, Michael J.
Organic Letters, 2010 , vol. 12, # 19 p. 4280 - 4283
123-75-1
+
1120-90-7
3-碘吡啶
→
反应条件
69698-09-5
反应条件
potassium phosphate; ethylene glycol; copper(l) iodide in isopropyl alcohol T=80°C; 14 h;
参考文献
Legault, Claude; Charette, Andre B.
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 7119 - 7122
首页
上一页
1
...
13
14
15
16
17
18
19
...
23
下一页
末页
到第
页
确定