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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-碘吡啶
合成路线
（共 228 条）
1120-90-7
3-碘吡啶
+
51934-41-9
对碘苯甲酸乙酯
→
反应条件
4385-71-1
4-吡啶-3-基-苯甲酸乙酯
反应条件
1: 3-iodo-pyridine With indium; n-tetradec-1l-ene; lithium chloride in tetrahydrofuran T=50°C; 5 h; 2: 4-iodobenzoic acid ethyl ester With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; 1-methyl-pyrrolidin-2-one 17 h; RefluxInert atmosphere;
参考文献
Chen, Yi-Hung; Knochel, Paul
Angewandte Chemie - International Edition, 2008 , vol. 47, # 40 p. 7648 - 7651
1120-90-7
3-碘吡啶
→
反应条件
4394-11-0
反应条件
1: EtMgBr / tetrahydrofuran / 0.42 h / Ambient temperature 2: 25 percent / tetrahydrofuran / 3 h View Scheme
参考文献
Furukawa, Naomichi; Shibutani, Tadao; Fujihara, Hisashi
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5845 - 5848
110-86-1
吡啶
+
1120-90-7
3-碘吡啶
→
反应条件
581-50-0
2,3'-联吡啶
+
4394-11-0
+
581-46-4
3,3'-联吡啶
反应条件
Br(1-)*C18H28N3(1+); sodium t-butanolate T=110°C; 4 h; Inert atmosphere;
参考文献
Chen, Wen-Ching; Hsu, Yu-Chen; Shih, Wei-Chun; Lee, Ching-Yu; Chuang, Wen-Han; Tsai, Yi-Fang; Chen, Peter Ping-Yu; Ong, Tiow-Gan
Chemical Communications, 2012 , vol. 48, # 53 p. 6702 - 6704
1120-90-7
3-碘吡啶
+
5720-05-8
4-甲基苯硼酸
→
反应条件
4423-09-0
3-(4-甲基苯基)吡啶
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; potassium carbonate; PdI2 in water; isopropyl alcohol T=80°C; Suzuki reaction; 5 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
1120-90-7
3-碘吡啶
+
108-88-3
甲苯
→
反应条件
4423-09-0
3-(4-甲基苯基)吡啶
+
90395-49-6
+
4385-67-5
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
110-91-8
+
1120-90-7
3-碘吡啶
+
201230-82-2
→
反应条件
492-85-3
反应条件
potassium phosphate; Pd((imidazolium)acetonaphthene)(allyl)Cl in toluene T=90°C; P=760.051 Torr; 19 h; Schlenk technique;
参考文献
Fang, Weiwei; Deng, Qinyue; Xu, Mizhi; Tu, Tao
Organic Letters, 2013 , vol. 15, # 14 p. 3678 - 3681
110-91-8
+
1120-90-7
3-碘吡啶
+
201230-82-2
→
反应条件
反应条件
triethylamine; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=50°C; P=750.075 Torr; 24 h;
参考文献
Takacs, Attila; Jakab, Balazs; Petz, Andrea; Kollar, Laszlo
Tetrahedron, 2007 , vol. 63, # 41 p. 10372 - 10378
1120-90-7
3-碘吡啶
+
14630-40-1
→
反应条件
50559-45-0
反应条件
pyrrolidine; copper(l) iodide; 4,4'-dichlorobenzophenone oxime derived palladacycle in 1-methyl-pyrrolidin-2-one T=110°C; sila-Sonogashira reaction; 8 h;
参考文献
Alonso, Diego A.; Botella, Luis; Najera; Pacheco, Ma. Carmen
Synthesis, 2004 , # 10 p. 1713 - 1718
1120-90-7
3-碘吡啶
+
80673-00-3
→
反应条件
50559-45-0
反应条件
tetrabutyl-ammonium chloride; sodium acetate; tris-(o-tolyl)phosphine; palladium diacetate in N,N-dimethyl-formamide T=100°C; Sonogashira coupling; 0.25 h; microwave irradiation;
参考文献
Sorensen, Ulrik S.; Pombo-Villar, Esteban
Tetrahedron, 2005 , vol. 61, # 10 p. 2697 - 2703
5029-67-4
+
1120-90-7
3-碘吡啶
→
反应条件
53159-76-5
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in butan-1-ol T=100°C; 5 h;
参考文献
Stabile, Paolo; Lamonica, Alessandro; Ribecai, Arianna; Castoldi, Damiano; Guercio, Giuseppe; Curcuruto, Ornella
Tetrahedron Letters, 2010 , vol. 51, # 24 p. 3232 - 3235
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