in neat (no solvent) heating (150-200°C), continuous removal of HNEt2; elem. anal.; mixt. of propadiene/propyne tris(trimethylastannyl)-derivatives (1:1) not separated;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 58, p. 2490 - 2491
Zhurnal Obshchei Khimii, , vol. 58, p. 2797 - 2798
in neat (no solvent)
byproducts: Me3SnI; heating (100-110°C, 2 h); fractional distn.; product mixt. not separated;
参考文献
Bogoradovskii, E. T.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 1038 - 1039
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 1167 - 1167
in tetrachloromethane
mixing at 0°C, heating for 30 min at 80°C; distn., overall yield 72percent;
参考文献
Bogoradovskii, E. T.; Zavgorodnii, V. S.; Liepin'sh, E. E.; Birgele, I. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1991 , vol. 61, p. 1295 - 1306
Zhurnal Obshchei Khimii, 1991 , vol. 61, p. 1418 - 1429
in neat (no solvent)
byproducts: Me3SnI; heating (100-110°C, 2 h); fractional distn.; product mixt. not separated;
参考文献
Bogoradovskii, E. T.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 1038 - 1039
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 1167 - 1167
