hydrogen; palladium on activated charcoal in acetic acid P=1520 - 2280 Torr; 80 h;
参考文献
Kelley, James L.; Krochmal, Mark P.; Linn, James A.; McLean, Ed W.; Soroko, Francis E.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 606 - 612
1: NaBH4 / ethanol / 16 h / Ambient temperature 2: SOCl2 / CH2Cl2 / 0.5 h 3: 22 percent / K2CO3 / dimethylformamide / 16 h / Ambient temperature 4: 63 percent / ethanol; H2O / 15 h / Ambient temperature 5: 61 percent / hydrogen / 5percent Pd/C / acetic acid / 80 h / 1520 - 2280 Torr View Scheme
参考文献
Kelley, James L.; Krochmal, Mark P.; Linn, James A.; McLean, Ed W.; Soroko, Francis E.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 606 - 612
1: SOCl2 / CH2Cl2 / 0.5 h 2: 22 percent / K2CO3 / dimethylformamide / 16 h / Ambient temperature 3: 63 percent / ethanol; H2O / 15 h / Ambient temperature 4: 61 percent / hydrogen / 5percent Pd/C / acetic acid / 80 h / 1520 - 2280 Torr View Scheme
参考文献
Kelley, James L.; Krochmal, Mark P.; Linn, James A.; McLean, Ed W.; Soroko, Francis E.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 606 - 612
Kelley, James L.; Krochmal, Mark P.; Linn, James A.; McLean, Ed W.; Soroko, Francis E.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 606 - 612
1: 22 percent / K2CO3 / dimethylformamide / 16 h / Ambient temperature 2: 63 percent / ethanol; H2O / 15 h / Ambient temperature 3: 61 percent / hydrogen / 5percent Pd/C / acetic acid / 80 h / 1520 - 2280 Torr View Scheme
参考文献
Kelley, James L.; Krochmal, Mark P.; Linn, James A.; McLean, Ed W.; Soroko, Francis E.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 606 - 612
