2-甲基-2-环己烯-1-酮合成路线 （共 131 条）
反应条件
stirring for 2 h; column chromy. (hexane/ether);
参考文献
Fujiwara, Jun; Sato, Tadashi
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1258 - 1264
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in 1-methyl-pyrrolidin-2-one T=90°C; 15 h; Molecular sieveInert atmosphere; regioselective reaction;
参考文献
Organic Letters, , vol. 14, # 4 p. 1172 - 1175
反应条件
copper(l) iodide; o-hydroxybenzoic acid ethyl ester equilibrium product ratio; further reagents, cycloalkenones; Product distribution;
参考文献
Krause, Norbert
Angewandte Chemie, 1994 , vol. 106, # 17 p. 1845 - 1847
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in 1-methyl-pyrrolidin-2-one T=90°C; 15 h; Molecular sieveInert atmosphere; regioselective reaction;
参考文献
Organic Letters, , vol. 14, # 4 p. 1172 - 1175
反应条件
1: methanol; aqueous hydrogen peroxide; aq. NaOH solution 2: BF3; benzene View Scheme
参考文献
House; Wasson
Journal of the American Chemical Society, 1957 , vol. 79, p. 1488,1490
反应条件
1.1: DIBAH / diethyl ether; toluene / 1 h / 0 °C 2.1: 0.9 g / pyridine / 20 °C 3.1: InCl3 / tetrahydrofuran / 1 h / 20 °C 3.2: PPh3 / Pd2dba3 / tetrahydrofuran / Heating View Scheme
参考文献
Baker, Lucas; Minehan, Thomas
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3957 - 3960
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 1639 - 1644
反应条件
1.1: DIBAH / diethyl ether; toluene / 1 h / 0 °C 2.1: 0.9 g / pyridine / 20 °C 3.1: InCl3 / tetrahydrofuran / 1 h / 20 °C 3.2: PPh3 / Pd2dba3 / tetrahydrofuran / Heating View Scheme
参考文献
Baker, Lucas; Minehan, Thomas
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3957 - 3960
反应条件
lithium carbonate; lithium chloride in N,N-dimethyl-formamide
T=200°C; 12 h;
参考文献
Lee, Junning; Snyder, John K.
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 4995 - 5008
反应条件
selenium(IV) oxide in dichloromethane
T=20°C; 48 h; Inert atmosphere;
参考文献
Hanessian, Stephen; Szychowski, Janek; Pablo Maianti
Organic Letters, 2009 , vol. 11, # 2 p. 429 - 432
