2-巯基吡啶-N-氧化物合成路线 （共 16 条）
反应条件
sodium sulfide; sodium hydrogensulfide in water T=95°C; 0.5 h;
参考文献
Zhong, Ping; Guo, Sheng-Rong; Song, Cai-Sheng
Synthetic Communications, 2004 , vol. 34, # 2 p. 247 - 253
反应条件
sodium carbonate; thiourea in water
反应条件
1: 80 percent / acetic acid; sodium acetate; trichloroisocyanuric acid / acetonitrile; CH2Cl2; H2O / 2 h / 40 °C 2: 94 percent / sodium sulfide; sodium hydrogen sulfide / H2O / 0.5 h / 95 °C View Scheme
参考文献
Synthetic Communications, , vol. 34, # 2 p. 247 - 253
反应条件
dicyclohexyl-carbodiimide in dichloromethane T=25°C; 10 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 41 p. 12261 - 12267
反应条件
pyridine; benzenesulfonyl chloride in dichloromethane Ambient temperature;
参考文献
Mahieu, Jean-Pierre; Gosselet, Martine; Sebille, Bernard; Beuzard, Yves
Synthetic Communications, 1986 , vol. 16, # 13 p. 1709 - 1722
参考文献
Newcomb, Martin; Marquardt, Donald J.
Heterocycles, 1989 , vol. 28, # 1 p. 129 - 132
反应条件
1: With 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in water T=110°C; 10 h; 2: With ethylenediamine in water T=20°C; 1 h;
参考文献
Kokatla, Hari Prasad; Thomson, Paul F.; Bae, Suyeal; Doddi, Venkata Ramana; Lakshman, Mahesh K.
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7842 - 7848
反应条件
dicyclohexyl-carbodiimide in dichloromethane T=25°C; 10 h;
参考文献
Ling, Taotao; Poupon, Erwan; Rueden, Erik J.; Kim, Sun H.; Theodorakis, Emmanuel A.
Journal of the American Chemical Society, 2002 , vol. 124, # 41 p. 12261 - 12267
反应条件
1: 81 percent / H2O2 / H2O / 1 h / 45 °C
2: HOAc / CH2Cl2 / 30 h / Ambient temperature
3: CH2Cl2; methanol / 72 h / Ambient temperature
View Scheme
参考文献
Barton, Derek H. R.; Chen, Chen; Wall, G. Michael
Tetrahedron, 1991 , vol. <32> 47, p. 6127 - 6138
反应条件
N-chloro-succinimide in water; benzene
参考文献
Colgate-Palmolive Company
Patent: US4049665 A1, 1977 ;
