2,4-二甲基环戊烷-1-酮合成路线 (共 3 条)
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Mironov,V.A.; Elizarova,A.N.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, # 8 p. 2731 - 2738,2688 - 2694
反应条件
trimethylsilyl trifluoromethanesulfonate 1.) THF, 0 deg C, 15 min; 2.) CH2Cl2, 15 min, 0 deg C; Yield given. Multistep reaction;
参考文献
Sato, Tadashi; Watanabe, Toshiyuki; Hayata, Toshihiro; Tsukui, Toru
Tetrahedron, 1989 , vol. 45, # 20 p. 6401 - 6408
反应条件
(2-pyrr)2Mg electrogenerated base in N,N,N',N',N'',N''-hexamethylphosphoric triamide; ethylene glycol dimethyl ether T=-50°C; 1.5 h; other temperatures, time, recyclization; Product distribution;
参考文献
Bonafoux, Dominique; Bordeau, Michel; Biran, Claude; Dunogues, Jacques
Synthetic Communications, 1998 , vol. 28, # 1 p. 93 - 98