1: isopropenyloxy trimethylsilane With methyllithium in tetrahydrofuran
T=0°C; Metallation;
2: cyclohept-2-en-1-one With ATPH in tetrahydrofuran; toluene
T=-78°C; Michael addition; 0.3 h;
参考文献
Saito, Susumu; Shimada, Itsuro; Takamori, Yusuke; Tanaka, Michiaki; Maruoka, Keiji; Yamamoto, Hisashi
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 7 p. 1671 - 1681