1,4-二甲基-2-碘苯合成路线 （共 37 条）
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C 2: sodium hydride; methyl malonic acid diethylester / N,N-dimethyl-formamide / 0.08 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 31 p. 10334 - 10342
反应条件
1: With N-methyl-2-(methylamino)ethylamine; copper(l) iodide in toluene T=110°C; 24 h; 2: With ammonia in N-dodecane; water; ethyl acetate; toluene T=25°C; 0.166667 h;
参考文献
MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Patent: WO2004/13094 A2, 2004 ;
Location in patent: Page 52-53 ;
参考文献
Kohlrausch; Pongratz
Monatshefte fuer Chemie, 1934 , vol. 64, p. 361,364, 365
Monatshefte fuer Chemie, 1935 , vol. 65, p. 6,14
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tris-(o-tolyl)phosphine; sodium t-butanolate in 1,4-dioxane T=100°C; 10.5 h;
参考文献
Wolfe, John P.; Buchwald, Stephen L.
Journal of Organic Chemistry, 1996 , vol. 61, # 3 p. 1133 - 1135
反应条件
carbon disulfide; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=100°C; 48 h; Inert atmosphereSealed tube;
参考文献
Zhao, Peng; Yin, Hang; Gao, Hongxin; Xi, Chanjuan
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5001 - 5006
反应条件
1: 67 percent / K2CO3; 18-crown-6 / Cu / 1,2-dichloro-benzene / 90 h / Heating 2: 50 percent / KOH / ethanol / 48 h / Heating View Scheme
参考文献
Plater, M. John; McKay, Murray; Jackson, Toby
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2695 - 2701
反应条件
sulfur dioxide; iodine; nitric acid; acetic acid T=220°C;
参考文献
Mascarelli; Longo
Gazzetta Chimica Italiana, 1941 , vol. 71, p. 297,299
Full Text Show Details
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 343
Full Text Show Details
Mascarelli; Longo
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1937 , vol. <6> 26, p. 292,296
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 121,127
参考文献
Klages; Liecke
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. <2> 61, p. 322
反应条件
bicyclo-[2.2.1]hept-2-ene; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=105°C; 48 h; Inert atmosphere;
参考文献
Della Ca', Nicola; Sassi, Giovanni; Catellani, Marta
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 14-15 p. 2179 - 2182
参考文献
Varma; Raman
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 245,247
