1: With N-benzyl-trimethylammonium hydroxide in tetrahydrofuran
T=20°C; Friedlaender condensation; 20 h;
2: With sodium hydroxide in ethanol; water
Heating;
参考文献
Fryatt, Tara; Pettersson, Hanna I.; Gardipee, Walter T.; Bray, Kurtis C.; Green, Stephen J.; Slawin, Alexandra M. Z.; Beall, Howard D.; Moody, Christopher J.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 7 p. 1667 - 1687
1.1: Triton B / tetrahydrofuran / 20 h / 20 °C
1.2: 0.2 g / NaOH / ethanol; H2O / Heating
2.1: 74 percent / potassium nitrosodisulfonate; sodium dihydrogen phosphate buffer / methanol / 20 °C / pH 6
View Scheme
参考文献
Fryatt, Tara; Pettersson, Hanna I.; Gardipee, Walter T.; Bray, Kurtis C.; Green, Stephen J.; Slawin, Alexandra M. Z.; Beall, Howard D.; Moody, Christopher J.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 7 p. 1667 - 1687
