Gil-Ramirez, Guzman; Karlen, Steven D.; Shundo, Atsuomi; Porfyrakis, Kyriakos; Ito, Yasuhiro; Briggs, G. Andrew D.; Morton, John J. L.; Anderson, Harry L.
Organic Letters, 2010 , vol. 12, # 15 p. 3544 - 3547
1.1: methanol / 1 h / 20 °C
1.2: 0.5 h / 0 - 20 °C
2.1: tetrahydrofuran; acetone; water / 2 h / 0 - 20 °C
3.1: phosphorous pentoxide / dichloromethane / 1 h / 20 °C / |Inert atmosphere
View Scheme
1: With copper(l) iodide; sodium azide; sodium L-ascorbate in ethanol; water
Inert atmosphere;
2: With N-methyl-2-(methylamino)ethylamine
1.5 h; RefluxInert atmosphere;
参考文献
De Miguel, Gustavo; Wielopolski, Mateusz; Schuster, David I.; Fazio, Michael A.; Lee, Olivia P.; Haley, Christopher K.; Ortiz, Angy L.; Echegoyen, Luis; Clark, Timothy; Guldi, Dirk M.
Journal of the American Chemical Society, 2011 , vol. 133, # 33 p. 13036 - 13054
