1: para-iodoanisole With copper; zinc in N,N-dimethyl-formamide T=125°C; 0.25 h; 2: 4-bromo-benzaldehyde With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=100°C; Negishi cross-coupling reaction; 0.25 h; Further stages.;
1: With sodium hydroxide; 1,3-dioctyl-benzimidazolium; bromide in water 0.5 h; Reflux; 2: With acetic acid in water 3: With FeCl3·6H2O in water pH=5 - 6; 7.5 h; Reflux;
参考文献
Bi, Xiaoxin; Wu, Lintao; Yan, Chaoguo; Jing, Xiaobi; Zhu, Hongxiang
Journal of the Chilean Chemical Society, 2011 , vol. 56, # 2 p. 663 - 664