您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴苯甲醛
合成路线
（共 1328 条）
1122-91-4
4-溴苯甲醛
→
反应条件
24133-54-8
反应条件
chromium dichloride; ethylenediamine in N,N-dimethyl-formamide T=-10°C; 2 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Avila-Sorrosa, Alcives; Vega-Ramirez, Leticia; Rodriguez-Dominguez, Rafael; Salgado-Zamora, Hector; Peralta-Cruz, Javier; Reyes-Arellano, Alicia
Chemistry Letters, 2010 , vol. 39, # 5 p. 500 - 501
1122-91-4
4-溴苯甲醛
→
反应条件
24133-54-8
反应条件
1: Mn / CrCl3 / tetrahydrofuran; dimethylformamide / 4 h / 65 °C 2: Bu4NF / tetrahydrofuran View Scheme
参考文献
Svatos, Ales; Boland, Wilhelm
Synlett, 1998 , # 5 p. 549 - 551
1122-91-4
4-溴苯甲醛
→
反应条件
873-75-6
4-溴苄醇
+
24133-54-8
反应条件
hydrogenchloride; samarium in tetrahydrofuran T=20°C; 32 h; Title compound not separated from byproducts;
参考文献
Talukdar; Fang
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 330 - 333
1122-91-4
4-溴苯甲醛
→
反应条件
24133-54-8
+
213776-05-7
+
384331-54-8
反应条件
manganese; TiCl2(THF)(4,6-(t-Bu2)C6H2O(2-{CH=N[(S)-CHBnCPh2O]}) in acetonitrile T=-10°C; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Sun, Jiangtao; Dai, Zhenya; Li, Changsi; Pan, Xu; Zhu, Chengjian
Journal of Organometallic Chemistry, 2009 , vol. 694, # 20 p. 3219 - 3221
1122-91-4
4-溴苯甲醛
+
7087-68-5
→
反应条件
873-75-6
4-溴苄醇
+
49678-04-8
+
24133-54-8
+
213776-05-7
反应条件
titanium tetrachloride in dichloromethane T=0 - 20°C; 30 h; Product distribution; Further Variations:ratio of reactants and reagent;
参考文献
Clerici, Angelo; Pastori, Nadia; Porta, Ombretta
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1825 - 1827
273-53-0
+
1122-91-4
4-溴苯甲醛
→
反应条件
27395-93-3
反应条件
PdCl(C3H5)(dppb); caesium carbonate in carbonic acid diethyl ester T=130°C; 17 h; Inert atmosphere; regioselective reaction;
参考文献
Dong, Jia Jia; Roger, Julien; Verrier, Cecile; Martin, Thibaut; Le Goff, Ronan; Hoarau, Christophe; Doucet, Henri
Green Chemistry, 2010 , vol. 12, # 11 p. 2053 - 2063
1122-91-4
4-溴苯甲醛
→
反应条件
2499-64-1
反应条件
1.1: triethylamine; Ph3P; Pd(OAc)2 / 2 h / Heating 2.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -10 - 20 °C 2.2: 81 percent / tetrahydrofuran; hexane / -20 - 20 °C 3.1: 88 percent / KOH / ethanol; tetrahydrofuran; H2O / 0 - 20 °C View Scheme
参考文献
Denmark, Scott E.; Neuville, Luc; Christy, Matthew E. L.; Tymonko, Steven A.
Journal of Organic Chemistry, 2006 , vol. 71, # 22 p. 8500 - 8509
1122-91-4
4-溴苯甲醛
→
反应条件
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 1 h / 23 °C / |Inert atmosphere 2: potassium hydroxide / tetrahydrofuran; methanol; water / 23 °C / |Inert atmosphere 3: 18-crown-6 ether; potassium hydroxide / dichloromethane / 4.5 h / -78 - 23 °C / |Inert atmosphere View Scheme
参考文献
Linseis, Michael; Zalis, Stanislav; Zabel, Manfred; Winter, Rainer F.
Journal of the American Chemical Society, 2012 , vol. 134, # 40 p. 16671 - 16692
1122-91-4
4-溴苯甲醛
+
4760-34-3
→
反应条件
2751-84-0
反应条件
oxygen; 1-hexadecylpyridinium bromide in water T=20°C; 0.75 h;
参考文献
Chakrabarty, Manas; Karmakar, Sulakshana; Mukherjee, Ratna; Arima, Shiho; Harigaya, Yoshihiro
Monatshefte fur Chemie, 2009 , vol. 140, # 4 p. 375 - 380
1122-91-4
4-溴苯甲醛
+
95-13-6
→
反应条件
30251-62-8
反应条件
potassium hydroxide in ethanol; toluene
参考文献
Bahner,C.T. et al.
Journal of Medicinal Chemistry, 1970 , vol. 13, p. 1240 - 1242
首页
上一页
1
...
37
38
39
40
41
42
43
...
133
下一页
末页
到第
页
确定
