(2S)-2-二乙氧基磷酰戊醛合成路线 （共 3 条）
参考文献
Teulade, Marie-Paule; Savignac, Philippe
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 405 - 408
反应条件
1: 1.) BuLi / 1) THF, hexane, -80 deg C, 15 min; 2) THF, hexane, -30 deg C --> room temperature
2: 1.) BuLi / 1) THF, hexane, -80 deg C, few minutes; 2) THF, hexane, -90 deg C, 15 min
3: aq. HCl / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Zanella, Yannick; Berte-Verrando, Sylvie; Diziere, Rachel; Savignac, Philippe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 22 p. 2835 - 2838
反应条件
1: 1.) BuLi / 1) THF, hexane, -80 deg C, few minutes; 2) THF, hexane, -90 deg C, 15 min
2: aq. HCl / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Zanella, Yannick; Berte-Verrando, Sylvie; Diziere, Rachel; Savignac, Philippe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 22 p. 2835 - 2838
