3,5-二甲基-4-硝基异噁唑合成路线 (共 36 条)
反应条件
sulfuric acid; nitric acid T=0 - 20°C;
参考文献
Zhang, Jinlong; Liu, Xihong; Ma, Xiaojuan; Wang, Rui
Chemical Communications, 2013 , vol. 49, # 81 p. 9329 - 9331
反应条件
in diethyl ether 24 h; Ambient temperature;
参考文献
Nesi, Rodolfo; Giomi, Donatella; Turchi, Stefania; Tedeschi, Piero; Ponticelli, Fabio
Gazzetta Chimica Italiana, 1993 , vol. 123, # 11 p. 633 - 636
反应条件
ammonium cerium(IV) nitrate in water; acetic acid 2 h; Ambient temperature;
参考文献
Fruttero, Roberta; Calvino, Rosella; Ferrarotti, Bruno; Gasco, Alberto; Aime, Silvio; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 523 - 530
反应条件
1: hydroxylamine 2: HNO3+H2SO4 View Scheme
参考文献
Journal of the Chemical Society, , vol. 119, p. 702
反应条件
1: hydroxylamine hydrochloride, sodium acetate trihydrate / H2O / 17 h / 5 °C 2: 20 percent / cerium(IV) ammonium nitrate / acetic acid; H2O / 2 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 523 - 530
反应条件
1: With piperidine in tetrahydrofuran T=70 - 80°C; 12 h; 2: With potassium permanganate in tetrahydrofuran; water; acetone T=20°C; Further stages.;
参考文献
Adamo, Mauro F.A.; Konda, Vivekananda R.; Donati, Donato; Sarti-Fantoni, Piero; Torroba, Tomas
Tetrahedron, 2007 , vol. 63, # 39 p. 9741 - 9745
反应条件
ammonium chloride; zinc in water T=0 - 5°C;
参考文献
Helvetica Chimica Acta, , vol. 74, # 3 p. 531 - 542
反应条件
piperidine in ethanol 24 h; Heating;
参考文献
Nesi; Giomi; Turchi; Tedeschi; Ponticelli
Synthetic Communications, 1992 , vol. 22, # 16 p. 2349 - 2355
反应条件
in ethanol 24 h; Heating;
参考文献
Nesi; Giomi; Turchi; Tedeschi; Ponticelli
Synthetic Communications, 1992 , vol. 22, # 16 p. 2349 - 2355
反应条件
1: With piperidine in tetrahydrofuran T=70 - 80°C; 12 h; 2: With potassium permanganate in tetrahydrofuran; water; acetone T=20°C; Further stages.;
参考文献
Adamo, Mauro F.A.; Konda, Vivekananda R.; Donati, Donato; Sarti-Fantoni, Piero; Torroba, Tomas
Tetrahedron, 2007 , vol. 63, # 39 p. 9741 - 9745