in neat (no solvent) byproducts: (CH3)3SnCl; (N2); cooling of PhSnCl3 in Schlenk flask to 0°C; addn. dropwise of SnMe4 with stirring; stirring for 0.5 h ((J. Org. Chem. 33 (1968) 1119); pumping under vac. at room temp. for several hs; GS-MS;
参考文献
Lloyd, Nicholas C.; Nicholson, Brian K.; Wilkins, Alistair L.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 12 p. 2757 - 2766
in tetrahydrofuran under Ar; a soln. of MeSn-contg. compd. (0.6 mmol) and PhSnCl3 (0.6 mmol) in THF was mixed; after 30 min in refluxing THF the solvent was removed in vac. and CD2Cl2was added; NMR spectra studies;
参考文献
Portnyagin, Ivan A.; Lunin, Valery V.; Nechaev, Mikhail S.
Journal of Organometallic Chemistry, 2008 , vol. 693, # 26 p. 3847 - 3850
