4-硝基吡啶-N-氧化物合成路线 （共 92 条）
反应条件
Durchleiten von Luft und Erwaermen des Reaktionsprodukts mit Wasser oder wss. Methanol;
参考文献
den Hertog et al.
Recueil des Travaux Chimiques des Pays-Bas, 1955 , vol. 74, p. 59,67
Full Text Show Details
Hayashi
Yakugaku Zasshi, 1950 , vol. 70, p. 145
Chem.Abstr., 1950 , p. 5881
反应条件
water; hydrogen bromide; urea T=160°C; In kleinem Mengen neben anderen Verbindungen,unter Druck.;
参考文献
Ochiai et al.
Yakugaku Zasshi, 1951 , vol. 71, p. 591,592
Chem.Abstr., 1952 , p. 980
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1422228 A1, 2004 ;
Location in patent: Page 201 ;
EP 1422228 A1
参考文献
den Hertog; Combe
Recueil des Travaux Chimiques des Pays-Bas, 1951 , vol. 70, p. 581,587
反应条件
tri-tert-butyl phosphine; palladium diacetate; potassium carbonate in toluene T=120°C; 24 h; Inert atmosphere;
参考文献
Duric, Sasa; Tzschucke, C. Christoph
Organic Letters, 2011 , vol. 13, # 9 p. 2310 - 2313
反应条件
potassium phosphate; tri-tert-butyl phosphine; palladium diacetate in toluene T=120°C; 24 h; Inert atmosphereGlovebox;
参考文献
Duric, Sasa; Sypaseuth, Fanni D.; Hoof, Santina; Svensson, Emma; Tzschucke, C. Christoph
Chemistry - A European Journal, 2013 , vol. 19, # 51 p. 17456 - 17463
反应条件
1: tri-tert-butyl phosphine; palladium diacetate; potassium carbonate / toluene / 24 h / 120 °C / Inert atmosphere 2: sodium tetrahydroborate; palladium on carbon / methanol / 22 h / Inert atmosphere View Scheme
参考文献
Duric, Sasa; Tzschucke, C. Christoph
Organic Letters, 2011 , vol. 13, # 9 p. 2310 - 2313
反应条件
titanium tetrachloride; tin(ll) chloride in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Kaczmarek, Lukasz; Balicki, Roman; Malinowski, Marek
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 3 p. 423 - 424
反应条件
cyclohexa-1,4-diene; 5-palladium/activated carbon in methanol T=120°C; 0.0833333 h; Microwave irradiation;
参考文献
Quinn, John F.; Bryant, Cole E.; Golden, Kathryn C.; Gregg, Brian T.
Tetrahedron Letters, 2010 , vol. 51, # 5 p. 786 - 789
反应条件
sodium hydroxide; zinc
参考文献
Ochiai; Katada
Yakugaku Zasshi, 1943 , vol. 63, p. 186,189
Chem.Abstr., 1951 , p. 5151
