ammonia in methanol Ambient temperature; Yield given;

1: ammonia / methanol / Ambient temperature 2: 71 percent / P4S10 / dioxane / 1 h / Heating 3: 70 mg / ethanol / 2 h / Heating 4: BF3*Et2O / 16 h / Ambient temperature 5: 87 percent / ammonia / methanol / 96 h / Ambient temperature View Scheme

1: 24 percent / ammonia / methanol / Ambient temperature 2: HCl / 1,2-dichloro-ethane / 4 h / 0 °C View Scheme

Multi-step reaction with 3 steps 1: 24 percent / ammonia / methanol / Ambient temperature2: 1.) NaH, 2.) NaI / 1.) dioxane, 2.) dioxane, reflux3: 35 percent / liq. H2S, 4-dimethylaminopyridine / 65 h / 50 °C  

Multi-step reaction with 5 steps 1: 24 percent / ammonia / methanol / Ambient temperature2: 1.) NaH, 2.) NaI / 1.) dioxane, 2.) dioxane, reflux3: 35 percent / liq. H2S, 4-dimethylaminopyridine / 65 h / 50 °C4: 70 mg / ethanol / 2 h / Heating5: 83 percent / ammonia / methanol / 96 h / Ambient temperature  

Multi-step reaction with 4 steps 1: ammonia / methanol / Ambient temperature2: 71 percent / P4S10 / dioxane / 1 h / Heating3: 70 mg / ethanol / 2 h / Heating4: BF3*Et2O / 16 h / Ambient temperature