2-乙酰基-1,4-苯醌合成路线 （共 30 条）
反应条件
in dichloromethane T=20°C; Michael addition; Title compound not separated from byproducts.;
参考文献
Benites, Julio; Valderrama, Jaime A.; Rivera, Felipe; Rojo, Leonel; Campos, Nair; Pedro, Madalena; Jose Nascimento, Maria Saeo
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 2 p. 862 - 868
反应条件
in acetonitrile dissolved acylquinone and allylstannane stood for 10 min under Ar; concentrated; column chromy. (silica gel); eluted (hexane/ether); NMR; IR; mass spectra; elem. anal.;
参考文献
Maruyama; Matano
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 3877 - 3885
反应条件
in benzene 72 h; Irradiation;
参考文献
Abdulla, Khalid A.; Abdul-Rahman, Azhar L.; Al-Hamdany, Ra'Ad; Al-Saigh, Zeki Y.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 3 p. 498 - 504
反应条件
in benzene 72 h; Irradiation;
参考文献
Abdulla, Khalid A.; Abdul-Rahman, Azhar L.; Al-Hamdany, Ra'Ad; Al-Saigh, Zeki Y.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 3 p. 498 - 504
反应条件
1: BF3*OEt2 / benzene 2: pyridine / xylene / 3 h / Heating 3: pyridine / 24 h / 20 °C 4: 43 percent / DDQ / benzene / 5 h / Heating View Scheme
参考文献
Molinari, Aurora; Oliva, Alfonso; Del Corral, Jose Ma. Miguel; Castro, Ma. Angeles; Araya, Claudia; Garcia-Gravalos, Ma. Dolores; San Feliciano, Arturo
Farmaco, 2004 , vol. 59, # 8 p. 651 - 656
反应条件
1: 70 percent / benzene / 7 h / Heating 2: trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Beddoes, Roy L.; Bruce, J. Malcolm; Finch, Harry; Heelam, Leslie M. J.; Hunt, Ian D.; Mills, Owen S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2670 - 2676
参考文献
Woroshzow; Mamaew
Sb. Statei Obshch. Khim., 1953 , p. 533,536
Chem.Abstr., 1959 , p. 925
反应条件
hydrogen azide in dichloromethane 0.5 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 17, # 9 p. 1077 - 1088
反应条件
in dichloromethane
T=20°C; Michael addition;
参考文献
Valderrama, Jaime A.; Gonzalez, M. Florencia; Colonelli, Pamela; Vasquez, David
Synlett, 2006 , # 17 p. 2777 - 2780
反应条件
silver(l) oxide in dichloromethane
参考文献
Valderrama, Jaime A.; Ibacache, Andrea; Rodriguez, Jaime A.; Theoduloz, Cristina; Benites, Julio
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 8 p. 3398 - 3409
