反应条件
1: trifluoroacetic acid / dimethylformamide / 120 h / Ambient temperature 2: 1.) 30percent H2O2, K2CO3 / 1.) water, RT, overnight, 2.) acetonitrile, reflux, 20 h 3: 80.3 percent / lithium aluminum hydride / tetrahydrofuran / a) RT, 18 h, b) reflux, 1 h 4: 1.) NaH / 1.) DMF, RT, 20 min, 2.) RT, overnight View Scheme
参考文献
Abushanab; Vemishetti; Leiby; Singh; Mikkilineni; Wu; Saibaba; Panzica
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2598 - 2602
