1-吡咯烷-1-环己烯合成路线 (共 146 条)
反应条件
1: dioxane / 3 h / Heating
2: 1.) LAH / 1.) ether, 0 deg C, then RT, 3 h, 2.) -15 deg C
View Scheme
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412
反应条件
1: (i) , (ii) aq. HCl
2: <PhCH2NMe3>OH / methanol
3: aq. HCl / acetic acid / Heating
View Scheme
参考文献
Fusco,R. et al.
Farmaco, Edizione Scientifica, 1965 , vol. 20, p. 393 - 407
反应条件
acetic acid in toluene
T=-78°C; 1 h;
参考文献
Momiyama, Norie; Yamamoto, Hisashi
Journal of the American Chemical Society, 2005 , vol. 127, # 4 p. 1080 - 1081
反应条件
1: Et3N / acetonitrile / 2 h / -10 °C
2: DMSO / 0.75 h
3: 6N HCl
View Scheme
参考文献
Barkallah, Salim; Boukraa, Mohamed; Zantour, Hedi; Baccar, Belgacem
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 108, # 1-4 p. 51 - 56
反应条件
(i), (ii) H2O; Multistep reaction;
参考文献
American Hoechst Corporation
Patent: US3997557 A1, 1976 ;
反应条件
(i), (ii) H2O; Multistep reaction;
参考文献
American Hoechst Corporation
Patent: US3997557 A1, 1976 ;
反应条件
(i), (ii) H2O; Multistep reaction;
参考文献
American Hoechst Corporation
Patent: US3997557 A1, 1976 ;
反应条件
(i), (ii) H2O; Multistep reaction;
参考文献
American Hoechst Corporation
Patent: US3997557 A1, 1976 ;
参考文献
American Hoechst Corporation
Patent: US3931407 A1, 1976 ;
反应条件
(i), (ii) H2O; Multistep reaction;
参考文献
American Hoechst Corporation
Patent: US3997557 A1, 1976 ;