1-吡咯烷-1-环己烯合成路线 （共 146 条）
反应条件
benzene Erwaermen des Reaktionsprodukts mit wss. Methanol;
参考文献
Segre et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3503
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Mondon
Chemische Berichte, 1959 , vol. 92, p. 1461,1469
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Boekelheide et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3955,3957
反应条件
in chloroform T=100°C; 1.5 h;
参考文献
Sugita, Teruyo; Koyama, Junko; Tagahara, Kiyoshi; Suzuta, Yukio
Heterocycles, 1985 , vol. 23, # 11 p. 2789 - 2792
反应条件
1)dioxane, reflux, 2) water; Yield given. Multistep reaction;
参考文献
Kuchar, Miroslav; Brunova, Bohumila; Grimova, Jaroslava; Vanecek, Stanislav; Holubek, Jiri
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 12 p. 2896 - 2908
反应条件
in 1,4-dioxane Heating;
参考文献
Harvey, Ronald G.; Pataki, John; Cortez, Cecilia; Raddo, Pasquale Di; Yang, ChengXi
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1210 - 1217
反应条件
1: With triethylamine in acetonitrile T=100°C; 12 h; 2: With water; acetic acid in acetonitrile 3 h; Heating / reflux;
参考文献
ABBOTT LABORATORIES
Patent: WO2007/118185 A2, 2007 ;
Location in patent: Page/Page column 50 ;
WO 2007/118185 A2
反应条件
(i) toluene, (ii) H2O; Multistep reaction;
参考文献
Stork,G. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 207 - 222
反应条件
triethylamine in toluene
T=-10 - 80°C; 18.67 h;
参考文献
Jones, Alan M.; Lorion, Magali M.; Lebl, Tomas; Slawin, Alexandra M.Z.; Philp, Douglas; Westwood, Nicholas J.
Tetrahedron, 2010 , vol. 66, # 51 p. 9667 - 9674
反应条件
triethylamine in toluene
1.) -5 to 5 deg C, 2 h; 2.) to RT, 0.5 h; 3.) heating, 4 h; 4.) RT, 12 h;
参考文献
Friary; Seidl; Schwerdt; Cohen; Hou; Nafissi
Tetrahedron, 1993 , vol. 49, # 33 p. 7169 - 7178
反应条件
1: 87 percent / dioxane / 1.5 h / Heating
2: LiAlH4 / diethyl ether / 0.5 h / Ambient temperature
3: aq. NaOH / 1 h / 100 °C
View Scheme
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412
反应条件
1,4-dioxane
anschliessend Erhitzen mit H2O;
参考文献
Stork
Patent: US2773099 , 1954 ;
