1-吡咯烷-1-环己烯合成路线 (共 146 条)
反应条件
hydroquinone in diethyl ether
参考文献
Aponick, Aaron; Li, Chuan-Ying; Biannic, Berenger
Organic Letters, 2008 , vol. 10, # 4 p. 669 - 671
反应条件
in 1,4-dioxane
16 h; Heating;
参考文献
Sielemann, Dirk; Keuper, Ralf; Risch, Nikolaus
Advanced Synthesis and Catalysis, 1999 , vol. 341, # 5 p. 487 - 491
反应条件
caesium carbonate in dichloromethane
24 h;
参考文献
Fioravanti, Stefania; Pellacani, Lucio; Tardella, Paolo A.
Gazzetta Chimica Italiana, 1997 , vol. 127, # 1 p. 41 - 44
反应条件
CaO in dichloromethane
24 h;
参考文献
Fioravanti, Stefania; Pellacani, Lucio; Tardella, Paolo A.
Gazzetta Chimica Italiana, 1997 , vol. 127, # 1 p. 41 - 44
反应条件
in toluene
48 h; Heating;
参考文献
Rigby, James H.; Balasubramanian, N.
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4569 - 4571
反应条件
1: Ambient temperature
2: toluene / Heating
View Scheme
参考文献
Rigby, James H.; Qabar, Maher
Synthetic Communications, 1990 , vol. 20, # 17 p. 2699 - 2709
反应条件
1: 70 percent / ethanol / 16 h
2: 100 percent / LiAlH4 / diethyl ether / 3 h / Ambient temperature
3: 68 percent / oxalic acid / dioxane / 6 h / Heating
View Scheme
参考文献
Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1980 , vol. 36, p. 3585 - 3590
反应条件
1: benzene / Erwaermen des Reaktionsprodukts mit wss. Methanol
View Scheme
参考文献
Mondon
Chemische Berichte, 1959 , vol. 92, p. 1461,1469
反应条件
1: With 9,10-dimethyl-9,10-dibora-9,10-dihydroanthracene in diethylene glycol dimethyl ether
T=90°C; electron-demand Diels-Alder reaction; 60 h;
2: With 3-chloro-benzenecarboperoxoic acid in diethylene glycol dimethyl ether
T=-78 - 20°C;
参考文献
Kessler, Simon N.; Neuburger, Markus; Wegner, Hermann A.
European Journal of Organic Chemistry, 2011 , # 17 p. 3238 - 3245
反应条件
benzyltriphenylphosphonium borohydride in methanol
T=20°C; 0.5 h;
参考文献
Hajipour; Mallakpour; Najafi
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 170, p. 197 - 203