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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
112575-87-8
合成路线
（共 6 条）
112575-86-7
→
反应条件
112575-87-8
反应条件
potassium hydroxide; ethylene glycol T=160°C; 6 h;
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio; Avigliano, Luciana; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 802 - 806
4518-10-9
3-氨基苯甲酸甲酯
→
反应条件
112575-87-8
反应条件
1: 65 percent / glacial acetic acid / 0.5 h / Heating 2: 73 percent / lithium aluminum hydride / diethyl ether / 3 h / Heating 3: 95 percent / phosphorus tribromide / diethyl ether / 4 h / Heating 4: 65 percent / aq. ethanol / 3 h / Heating 5: 71 percent / potassium hydroxide, ethylene glycol / 6 h / 160 °C View Scheme
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio; Avigliano, Luciana; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 802 - 806
112596-36-8
1-(3-溴甲基)苯基-吡咯
→
反应条件
112575-87-8
反应条件
1: 65 percent / aq. ethanol / 3 h / Heating 2: 71 percent / potassium hydroxide, ethylene glycol / 6 h / 160 °C View Scheme
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio; Avigliano, Luciana; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 802 - 806
83140-94-7
[3-(1H-吡咯-1-基)苯基]甲醇
→
反应条件
112575-87-8
反应条件
1: 95 percent / phosphorus tribromide / diethyl ether / 4 h / Heating 2: 65 percent / aq. ethanol / 3 h / Heating 3: 71 percent / potassium hydroxide, ethylene glycol / 6 h / 160 °C View Scheme
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio; Avigliano, Luciana; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 802 - 806
83140-93-6
1-(3-乙氧基羰基苯基)吡咯
→
反应条件
112575-87-8
反应条件
1: 73 percent / lithium aluminum hydride / diethyl ether / 3 h / Heating 2: 95 percent / phosphorus tribromide / diethyl ether / 4 h / Heating 3: 65 percent / aq. ethanol / 3 h / Heating 4: 71 percent / potassium hydroxide, ethylene glycol / 6 h / 160 °C View Scheme
参考文献
Artico, Marino; Corelli, Federico; Massa, Silvio; Stefancich, Giorgio; Avigliano, Luciana; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 802 - 806
2437-43-6
+
124-38-9
二氧化碳
→
反应条件
112575-87-8
反应条件
1: 1-m-tolyl-1H-pyrrole With n-butyllithium; potassium tert-butylate in tetrahydrofuran T=-75°C; 1 h; 2: carbon dioxide in tetrahydrofuran T=-75°C;
参考文献
Faigl, Ferenc; Thurner, Angelika; Vass, Bernadett; Toke, Laszlo
Journal of Chemical Research - Part S, 2003 , # 3 p. 132 - 133
