N,N-二甲基-2-苯乙胺合成路线 (共 89 条)
反应条件
1: With titanium(IV) isopropylate in methanol T=20°C; Addition; 2: With sodium tetrahydroborate in methanol T=20°C; Reduction; 1.5 h;
参考文献
Synthetic Communications, , vol. 30, # 11 p. 2001 - 2008
反应条件
formic acid in water T=0 - 100°C; 10 h; Inert atmosphere;
参考文献
Chemical Communications, , # 31 p. 4678 - 4680
反应条件
NiCuFeO(x) in anhydrous xylene 24 h; Inert atmosphereSealed tubeReflux;
参考文献
Chemistry - A European Journal, , vol. 19, # 11 p. 3665 - 3675
反应条件
sodium tetrahydroborate in tetrahydrofuran; trifluoroacetic acid T=25°C; 24 h;
参考文献
Synthesis, , # 8 p. 709 - 711
反应条件
ammonia; sodium in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 25, # 10 p. 2689 - 2691
反应条件
di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine in tetrahydrofuran T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 47, # 28 p. 4871 - 4875
参考文献
Journal of Organic Chemistry, , vol. 64, # 3 p. 807 - 818
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; cesium fluoride 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 55, # 9 p. 2767 - 2770
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 0.5 h; Heating;
参考文献
Tetrahedron Letters, , vol. 26, # 44 p. 5367 - 5370
反应条件
zinc in acetonitrile 1) cooling with an ice-salt bath -> room temperature, 5 h, 2) room temp., 2 days;
参考文献
Journal of Organic Chemistry, , vol. 48, # 10 p. 1621 - 1628