N,N-二甲基-2-苯乙胺合成路线 (共 89 条)
反应条件
1: (i) nBuLi, THF, (ii) /BRN= 1761302/ 2: LiAlH4 / tetrahydrofuran 4: H2 / Pd-C / ethanol View Scheme
参考文献
Synthetic Communications, , vol. 3, p. 325 - 332
反应条件
2: H2 / Pd-C / ethanol View Scheme
参考文献
Synthetic Communications, , vol. 3, p. 325 - 332
反应条件
1: LiAlH4 / tetrahydrofuran 3: H2 / Pd-C / ethanol View Scheme
参考文献
Synthetic Communications, , vol. 3, p. 325 - 332
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3933
反应条件
cesium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide 44 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 52, # 9 p. 1844 - 1847
反应条件
sodium hydrogencarbonate in methanol; water T=20°C;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 41, # 1 p. 53 - 61
反应条件
carbon dioxide T=130°C; P=30752.5 Torr; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 7 p. 2771 - 2777
反应条件
ethanol; palladium Hydrogenation;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 271, p. 439,445
Journal of the American Chemical Society, , vol. 60, p. 1789,1790
反应条件
methanol; sodium methylate
参考文献
Journal of the American Chemical Society, , vol. 32, p. 769
反应条件
sulfuric acid T=30 - 40°C; Electrolysis.an Bleikathoden;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 431, p. 213
Chem. Zentralbl., , vol. 94, # II p. 403